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EPA Method 23-Determination of Polychlorinated Dibenzo-p-Dioxins and Polychlorinated Dibenzofurans From Stationary Sources

FR Abstract
This action finalizes editorial and technical revisions to the Environmental Protection Agency's (EPA's) Method 23 (Determination of Polychlorinated Dibenzo-p-Dioxins, Polychlorinated Dibenzofurans, and Polycyclic Aromatic Hydrocarbons from Stationary Sources). Final revisions include incorporating true, comprehensive, and stable isotope dilution for quantifying target compounds using corresponding carbon-13 labeled compounds for each target compound including most of the polycyclic aromatic hydrocarbons (PAH) and changing the method quality control from the current prescriptive format to a more flexible performance-based approach with specified performance criteria. We are also finalizing revisions that expand the list of target compounds of Method 23 to include PAH and polychlorinated biphenyls (PCB). The final revisions allow facilities and their test teams flexibility when sampling and measuring polychlorinated dibenzo-p-dioxins and polychlorinated dibenzofurans (PCDD/PCDF), PAH, and PCB from stationary sources with a comprehensive isotope dilution method while ensuring that the stack testing community can consistently implement the method across emissions sources and facilities.
Incorporation
FR Document Number
2023-04958
Federal Register Volume
88
Federal Register Year
2023-03-20
Federal Register Start Page
16732
Federal Register End Page
16774
CFR Citation
40 CFR 63
FR Citation
88 FR 16732
CFR title
40
CFR Part
63
Document Number
ASTM D6911-15
Document Edition
2016
Standard Title
Standard Guide for Packaging and Shipping Environmental Samples for Laboratory Analysis
Excerpts
made in response to comments. III. Incorporation by Reference The EPA is incorporating by reference American Society for Testing and Materials (ASTM) … Dibenzofurans emissions from Stationary Sources, EPA Publication SW-846 (incorporated by reference—see § 63.14); or (B) Method 23, provided in Appendix A, Part … Emissions from Stationary Sources, EPA Publication SW-846, as incorporated by reference in § 260.11 of this chapter or Method 23, provided in Appendix
Record Source
www.federalregister.gov